Current research projects

Image Reducing the filling quantity
Image Multifunctional electronic modules for cryogenic applications
Image Behavior of multiphase cryogenic fluids
Image ZeroHeatPump
Image Low noise and non metallic liquid-helium cryostat
Image Energy efficiency consulting - cogeneration systems
Image Software for technical building equipment
Image Modular storage system for solar cooling
Image Cryostats, Non-Metallic and Metallic
Image Laseroptical measurement
Image Lifetime prediction of hermetic compressor systems
Image IO-Scan - Integral measuring optical scanning method
Image Characterisation of Superconductors in Hydrogen Atmosphere
Image Brine (water)-water heat pump
Image Non- invasive flow measurements
Image High temperature heat pump

You are here:  Home /  Measurements and Tests


Mass Spectrometer

Industrie und Forschungsinstitute

Gunar Schroeder

+49-351-4081-5129

Determining the composition of gas mixtures in the high or ultra-high vacuum range

Mass spectrometry is a method for determining the composition of gas mixtures in the high or ultra-high vacuum range. It can be used to carry out qualitative and quantitative gas analyses and leak detection or to determine trace contamination.

The individual neutral gas particles are ionized by an electron impact ion source and separated from each other in an electric quadrupole field according to their mass-to-charge ratio. The filtered ions are then recorded by a detector. The ion current detected is proportional to the partial pressure of the respective gas component. For a more precise quantitative gas analysis, the relatively operating measuring instrument can be calibrated with a calibration gas.

The test set-up consists of a test chamber with a connected turbo-molecular-pump and fore vacuum pump. The mass spectrometer requires a vacuum <1,5×10-7 psi (<1×10-5 mbar) to be able to measure with high precision. The mass spectrometer and a vacuum sensor are mounted on the test chamber. The mass spectrometer is connected to a measuring PC with corresponding software.

Available measurement modes are:

  • Vacuum analysis, to determine residual gas components, evaluation as a plot of ion current and mass
  • Leak detection, with helium or another tracer gas, the ion current of the tracer gas or the corresponding mass is recorded and plotted over the time
  • Mass spectrum, evaluation of ion current and mass with user-defined specifications and time trend
Paramter Test value
Analysis Vacuum analysis, leak detection, mass spectrum, trace contamination
Detectable gases H2, He, N2, H2O, O2, CO2 usw.
Mass range 1 – 100 Da (1,66×10-27 – 1,66×10-25 kg)
Detection limit 1.5×10-15 psi / 3×10-13 mbar
Min. vacuum pressure and max. temperature range <7.3×10-6 psi / 5×10-4 mbar, < 150°C / 302°F

[Translate to EN:]


Your Request

Further Projects - Measurements and Tests

Image

Testzentrum PLWP at ILK Dresden

Test Fluid-Energy Machines and Components

Image

Performance tests of refrigerant compressors

Does your compressor perform well?

Image

Measurement of insulated packaging

How efficient is my cool box?

Image

Cold meter

The fast way to refrigerating capacity

Image

Verification of storage suitability of cryo tubes

Artificial aging of primary packaging for biobanking applications